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Multiphase Homogeneous Catalysis, Vol 1
Multiphase Homogeneous Catalysis, Vol 1
Date: 14 April 2011, 01:42

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This book describes for the first time all homogeneously catalyzed reactions in multiphase operation. Thus it summarizes the progress which became possible by the introduction of separate phases in the context of “homogeneous” catalysis: an apparent contradiction with far-reaching consequences. The book reviews all the realistic possibilities described so far using multiphase operation of homogeneous catalysis: processes with organic/organic, organic/aqueous, or “fluorous” solvent pairs (solvent combinations), nonaqueous ionic solvents, supercritical fluids, and systems with soluble polymers. The accounts concentrate on the modification and the handling of homogeneous catalysts under multiphase conditions in general, and the removal and subsequent recycling of the catalyst in particular. Why multiphase systems? This goes back to the 1980s and the enormous impetus which was given to the homogeneous catalysis community by the first realization of Ruhrchemie/Rhone-Poulenc’s aqueous-phase oxo process at the Oberhausen plant site. Astonishingly, this fact (and not the earlier SHOP process of Shell) sensitized the scene to the possibilities of multiphase action to imitate the decisive advantage of heterogeneous catalysis: the immediate separation of catalyst and substrates/products just after reaction which makes it possible to avoid additional separation steps post-reaction, such as distillations and other thermally stressing procedures.

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