Advanced Organic Synthesis METHODS AND TECHNIQUES - ISBN:0075165531

Advanced Organic Synthesis METHODS AND TECHNIQUES

Date: 28 April 2011, 04:51

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Library of Congress Catalog Card Number: 75-165531
The purpose of this text is to provide a survey, and systematic introduction to, the
modern techniques of organic synthesis for the advanced undergraduate student or the
beginning graduate student. An attempt has been made to acquaint the student with a
variety of laboratory techniques as well as to introduce him to chemical reagents that
require deftness and care in handling. Experiments have been drawn from the standard
literature of organic synthesis including suitable modifications of several of the reliable
and useful preparations that have appeared in "Organic Synthesis," Other examples
have been drawn from the original literature. Where ever possible, the experiments have
been adapted to the locker complement commonly found in the advanced synthesis
course employing intermediate scale standard taper glassware. Special equipment for
the performance of some of the syntheses would include low-pressure hydrogenation
apparatus, ultraviolet lamps and reaction vessels. Dry Ice (cold finger) condensers,
vacuum sublimation and distillation apparatus, and spectroscopic and chromato-
graphic instruments. In general, an attempt has been made to employ as substrates
materials that are available commercially at reasonable cost, although several of the
experiments require precursor materials whose preparation is detailed in the text. Some
of the reagents are hazardous to handle, but I believe that, under reasonable supervision,
advanced students will be able to perform the experiments with safety.

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